Synthesis of Graphene Oxide by Modified Hummers Method and Hydrothermal Synthesis of Graphene-NiO Nano Composite for Supercapacitor Application

ثبت نشده
چکیده

Graphene oxide was synthesized by using modified Hummers method and also Graphene-NiO nanocomposite prepared by hydrothermal method with the use of graphene oxide solution, Ni(NO3)2•6H2O and urea as raw materials. The synthesized nanocomposite was characterized by the XRD, Raman, SEM, TGA and energy dispersive spectrometer analysis. The results demonstrate that NiO nano particles uniformly covered on the surface of the graphene layer and Raman spectroscopy states that well formation of the Graphene-NiO Nano composite. CV curves of Graphene-NiO electrodes at different scan rates conveys that capacitance characteristic is very different from that of traditional electric double-layer capacitance in which the shape is normally an ideal rectangular shape. Therefore, cyclic voltammetry analysis is the evidence of these materials are having the ability of supercapacitor electrode material properties. TGA Analysis is used for the estimation of how much of graphene is exist in the Graphene-NiO nanocomposite. *Corresponding author: Narasimharao K, Sreenidhi Institute of Science and Technology, Ghatkesar, Hyderabad 500130, Telangana, India, Tel: 08415200595; E-mail: [email protected] Received August 11, 2016; Accepted September 26, 2016; Published October 06, 2016 Citation: Narasimharao K, Venkata Ramana G, Sreedhar D, Vasudevarao V (2016) Synthesis of Graphene Oxide by Modified Hummers Method and Hydrothermal Synthesis of Graphene-NiO Nano Composite for Supercapacitor Application. J Material Sci Eng 5: 284. doi:10.4172/2169-0022.1000284 Copyright: © 2016 Narasimharao K, et al. This is an open-access article distributed under the terms of the Creative Commons Attribution License, which permits unrestricted use, distribution, and reproduction in any medium, provided the original author and source are credited.

برای دانلود متن کامل این مقاله و بیش از 32 میلیون مقاله دیگر ابتدا ثبت نام کنید

ثبت نام

اگر عضو سایت هستید لطفا وارد حساب کاربری خود شوید

منابع مشابه

Evaluating the Effect of Graphite Source and Operating Conditions on the Synthesis of Graphene Oxide

In this research graphene oxide was synthesized by two methods. These methods were achieved by changing the improved Hummers’ and modified Hummers’ methods. Structure of graphene oxide was characterized by scanning electron microscopy (SEM) images, X-ray diffraction (XRD) patterns, Raman spectroscopy and Fourier transform infrared (FTIR) spectra. According to SEM image, the thickness of graphen...

متن کامل

Synthesis of graphene oxide / polydopamine composite for coating on clay substrate for water treatment

Water purification is a vital and essential thing for human life. The presence of pollutants in water is a major threat to the environment and human health. Various materials have been proposed and used for water treatment in recent years. Recent research has shown the potential of two-dimensional materials such as graphene oxide and its composites for water purification. The goal of this proje...

متن کامل

Synthesis of graphene oxide-Melamine – TioOxalic acid nanocomposite and its application in the elimination of Mercury (II) ions

In this study a new method by Application of graphene oxide Nano sheets– Melamine –TioOxalic acid composite was exhibited as adsorbent for the elimination of toxic mercury (II) ions from aqueous solutions. The combine has the authority to adsorb the organic and inorganic combines. Through the immobilization of Melamine-TioOxalic acid (MTO) onto graphene oxide nanosheets, the desired composite w...

متن کامل

Synthesis and characterization of Graphene Oxide in suspension and powder forms by chemical exfoliation method

In this study, an efficient and facile technique for preparing graphene oxide in suspension and powder forms was presented based on a modification on Hummers' method followed by an additional ultrasonic process. The method involved the provision of graphene oxide from graphite by reaction of potassium permanganate and sulfuric acid with stabilizing the medium complex. Furthermore, this study ev...

متن کامل

Synthesis and characterization of Graphene Oxide in suspension and powder forms by chemical exfoliation method

In this study, an efficient and facile technique for preparing graphene oxide in suspension and powder forms was presented based on a modification on Hummers' method followed by an additional ultrasonic process. The method involved the provision of graphene oxide from graphite by reaction of potassium permanganate and sulfuric acid with stabilizing the medium complex. Furthermore, this study ev...

متن کامل

ذخیره در منابع من


  با ذخیره ی این منبع در منابع من، دسترسی به آن را برای استفاده های بعدی آسان تر کنید

برای دانلود متن کامل این مقاله و بیش از 32 میلیون مقاله دیگر ابتدا ثبت نام کنید

ثبت نام

اگر عضو سایت هستید لطفا وارد حساب کاربری خود شوید

عنوان ژورنال:

دوره   شماره 

صفحات  -

تاریخ انتشار 2016